分析海水魚魚肉中總汞和甲基汞含量的一種新方法

Abstract： In this work we have developed a cost-effectivemethod for the analysis of methyl mercury (MeHg) inseawater fish muscle. The novelty of this method lies in theuse of microwave- assistedextraction with acidic solution (HCl), addition of toluene, and subsequent extraction with cysteine acetate solution where only MeHg is present because of its affinity for cysteine groups. MeHg in cysteine phase and total mercury in the homogenate muscle tissue were determined using a direct Hg analyzer (DMA-80). Validation, precision, and accuracy of the methodwere evaluated and monitored with a tuna fish certified reference material (CRM 463) containing MeHg. 

Keywords： Methyl mercury ；Microwave extraction；Mercury； Direct mercury analyzer