色譜柱： C18 （100*2.1mm, 5um）
流動相： A. Water (5mM乙酸胺+0.1%甲酸)， B. 甲醇。梯度洗脫：0－3min， 20％B->80%B, 3-7min, 80%B, 7.1-8min, 20%B.(您實驗室的液相系統，該提督方法要做相應的修改)
流速： 0.25mL/min.
質譜方法： ESI（+）,
|
Ion source: |
ESI |
|
Ion polarity: |
Positive |
|
Spray voltage: |
4800 V |
|
Sheath gas pressure: |
35 |
|
Auxiliary gas pressure: |
6 |
|
Ion transfer capillary temperature: |
350 C |
|
Source CID: |
0 |
|
Scan Type: |
SRM |
|
Q1 peak width |
0.7 Da in SRM |
|
Collision Pressure: |
Ar at 1.5 mTorr |
SRM transitions：
Last modified: 9/11/2007 16:43:25 PM by feiliu
Duration (min) 8.00
Tune Method D:\methods\nitrofuran\SEM-07-07-05.TSQTune
Q2 Gas Pressure: 1.5
1: + c SRM Micro Scans 1,
Parent Center Width Time CE Q1 PW Q3 PW Tube Lens
236.000 104.200 0.010 0.050 19 0.70 0.70 85
236.000 134.000 0.010 0.050 13 0.70 0.70 85
240.000 134.000 0.010 0.050 12 0.70 0.70 85
2: + c SRM Micro Scans 1,
Parent Center Width Time CE Q1 PW Q3 PW Tube Lens
209.000 165.900 0.010 0.050 12 0.70 0.70 78
209.000 191.900 0.010 0.050 10 0.70 0.70 78
212.000 168.000 0.010 0.050 11 0.70 0.70 78
3: + c SRM Micro Scans 1,
Parent Center Width Time CE Q1 PW Q3 PW Tube Lens
249.000 104.200 0.010 0.050 20 0.70 0.70 88
249.000 134.000 0.010 0.050 12 0.70 0.70 88
252.000 134.000 0.010 0.050 15 0.70 0.70 88
4: + c SRM Micro Scans 1,
Parent Center Width Time CE Q1 PW Q3 PW Tube Lens
335.000 262.000 0.010 0.050 16 0.70 0.70 78
335.000 291.000 0.010 0.050 10 0.70 0.70 78
340.000 296.000 0.010 0.050 11 0.70 0.70 78
